HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → HCID 70094067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | HCID 53963569 | HCID 53963569 | — |
| Product | HCID 70094067 | HCID 70094067 | 88.3% |
Reaction Steps
In the same manner as described in Example 9, 0.699 g (2.0 mmol) of the product of Example 62 and 0.295 g (2.4 mmol) of 1-bromopropane provided 0.691 g (88%) of the desired product as a yellow gum after preparative TLC eluting with 1:3 EtOAc:hexane. Electrospray Mass Spec 392.2(M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929097 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-6a5d9965dd4a4d7b8204d2cb880b9d9e |
| Source note | uspto-grants-1999_07 |