HCID 70094067, compound → HCID 21310869, compound

HRID 583326Notes

Reaction equation

HRID 583326 reaction equation
C[O:2][C:3](=[O:27])[C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:16]([C:19]1[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[CH:21][CH:20]=1)(=[O:18])=[O:17])[CH2:13][CH2:14][CH3:15]>CCOCC.CCCCCC>[CH3:26][O:25][C:22]1[CH:23]=[CH:24][C:19]([S:16]([N:12]([CH2:13][CH2:14][CH3:15])[C:5]2[C:6]([CH3:11])=[CH:7][C:8]([CH3:10])=[CH:9][C:4]=2[C:3]([OH:27])=[O:2])(=[O:18])=[O:17])=[CH:20][CH:21]=1

Participants

3

Reactant 1

HCID 70094067HCID 70094067, compound

Product 1

HCID 21310869HCID 21310869, compoundYield 79.3%

Reagents, catalysts & solvents 1

HCID 21584099Diethylether hexaneSolvent

Procedure

In the same amn as described in Example 109, 0.602 g (1.54 mmol) of the product of Example 105 provided 0.461 g (79%) of the desired carboxylic acid as a white solid after trituration with ether/hexane. Electrospray Mass Spec 378.2(M+H).

Sources & evidence

ORD record
ord-1771a037cd2c41588f9f3a52188f6992
Source dataset
uspto-grants-1999_07
Patent number
US05929097

Reaction notes

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