HRID583361

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID95114

2-Propenamide, N,N-di-2-propenyl-

C9H13NO

结构：COC(=O)c1cc(Br)cc(C)c1N(Cc1cccnc1)S(=O)(=O)c1ccc(OC)cc1

HCID70053864

未命名化合物

PRODUCTS

生成物

结构：C=CCN(CC=C)C(=O)C=Cc1cc(C)c(N(Cc2cccnc2)S(=O)(=O)c2ccc(OC)cc2)c(C(=O)OC)c1

HCID70054299

未命名化合物

收率 53.7%

PROCEDURE

实验过程

In the same manner as described in Example 203, 550.4 mg (1.0 mmol) of the product of Example 89 and 453.6 mg (3.0 mmol) of N,N-diallylacrylamide provided 309 mg (53%) of the desired product as a yellow gum. Electrospray Mass Spec 576(M+H).

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-c2edf6d078ad49e789bbb522a4a89f22
来源数据集: uspto-grants-1999_07
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05929097
来源说明: uspto-grants-1999_07

反应 SMILES

[CH3:1][O:2][C:3](=[O:31])[C:4]1[CH:9]=[C:8](Br)[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:20]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1)(=[O:22])=[O:21])[CH2:13][C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1.[CH2:32]([N:35]([CH2:40][CH:41]=[CH2:42])[C:36](=[O:39])[CH:37]=[CH2:38])[CH:33]=[CH2:34]>>[CH3:1][O:2][C:3](=[O:31])[C:4]1[CH:9]=[C:8]([CH:38]=[CH:37][C:36](=[O:39])[N:35]([CH2:32][CH:33]=[CH2:34])[CH2:40][CH:41]=[CH2:42])[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:20]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1)(=[O:22])=[O:21])[CH2:13][C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1