2-Propenamide, N,N-di-2-propenyl- → HCID 70054299, compound

HRID 583361Notes

Reaction equation

HRID 583361 reaction equation
[CH3:1][O:2][C:3](=[O:31])[C:4]1[CH:9]=[C:8](Br)[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:20]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1)(=[O:22])=[O:21])[CH2:13][C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1.[CH2:32]([N:35]([CH2:40][CH:41]=[CH2:42])[C:36](=[O:39])[CH:37]=[CH2:38])[CH:33]=[CH2:34]>>[CH3:1][O:2][C:3](=[O:31])[C:4]1[CH:9]=[C:8]([CH:38]=[CH:37][C:36](=[O:39])[N:35]([CH2:32][CH:33]=[CH2:34])[CH2:40][CH:41]=[CH2:42])[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:20]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1)(=[O:22])=[O:21])[CH2:13][C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1

Participants

3

Reactant 2

HCID 951142-Propenamide, N,N-di-2-propenyl-HCID 70053864HCID 70053864, compound

Product 1

HCID 70054299HCID 70054299, compoundYield 53.7%

Procedure

In the same manner as described in Example 203, 550.4 mg (1.0 mmol) of the product of Example 89 and 453.6 mg (3.0 mmol) of N,N-diallylacrylamide provided 309 mg (53%) of the desired product as a yellow gum. Electrospray Mass Spec 576(M+H).

Sources & evidence

ORD record
ord-c2edf6d078ad49e789bbb522a4a89f22
Source dataset
uspto-grants-1999_07
Patent number
US05929097

Reaction notes

Loading…