HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorothiophene-2-boronic acid → HCID 70055239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorothiophene-2-boronic acid | HCID 2734324 | — |
| Reactant | HCID 70053864 | HCID 70053864 | — |
| Product | HCID 70055239 | HCID 70055239 | 61.1% |
Reaction Steps
In the same manner as described in Example 241, 505 mg (1.0 mmol) of the product of Example 89 and 357 mg (2.2 mmol) of 5-chlorothiophene-2-boronic acid provided 332 mg (61%) of the desired product as an yellow solid. Electrospray Mass Spec 543 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929097 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-3e22dd78188749399b9589edfe05a710 |
| Source note | uspto-grants-1999_07 |