HCID 54241089, compound → HCID 70055465, compound

HRID 583377Notes

Reaction equation

HRID 583377 reaction equation
[CH2:1]([O:8][C:9](=[O:30])[C:10]1[C:15]([CH3:16])=[CH:14][CH:13]=[C:12]([CH3:17])[C:11]=1[NH:18][S:19]([C:22]1[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[CH:24][CH:23]=1)(=[O:21])=[O:20])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>CCCCCC>[CH2:1]([O:8][C:9](=[O:30])[C:10]1[C:15]([CH3:16])=[CH:14][CH:13]=[C:12]([CH3:17])[C:11]=1[N:18]([CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[S:19]([C:22]1[CH:23]=[CH:24][C:25]([O:28][CH3:29])=[CH:26][CH:27]=1)(=[O:21])=[O:20])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 1

HCID 54241089HCID 54241089, compound

Product 1

HCID 70055465HCID 70055465, compoundYield 183.1%

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

In the same manner as described in Example 9, 321 mg (0.754 mmol) of the product of Example 287 provided 356 mg (92%) of the desired product as a white solid after trituration with hexane. Electrospray Mass Spec 516 (M+H).

Sources & evidence

ORD record
ord-2671d97788e447058c5b296934bf356a
Source dataset
uspto-grants-1999_07
Patent number
US05929097

Reaction notes

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