2,2'-Dithiodibenzoyl chloride → 2,2'-Dithiobis[N-[4-nitro-3-(trifluoromethyl)phenyl]benzamide]

Participants

Reaction Steps

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 4-nitro-3-(trifluoromethyl)aniline (2.39 g, 11.6 mmol) in 19 mL of pyridine. The crude product was recrystallized from ethyl ether to yield 0.25 g of the title compound, mp 167-169° C.

Provenance & Evidence