反应详情

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.00 g, 2.92 mmol) in 20 mL of dichloromethane and 4-fluoroaniline (0.657 g, 5.91 mmol) in 5 mL of pyridine. The crude product was triturated with hot ethanol-ethyl acetate mixture, filtered, and recrystallized from ethanol-DMF to yield 0.14 g of the title compound, mp 242-244° C.

1. customThis compound was prepared
2. customThe crude product was triturated with hot ethanol-ethyl acetate mixture
3. filtrationfiltered
4. customrecrystallized from ethanol-DMF