Triethylamine → [2-[[2-(Pyrrolidine-1-carbonyl)phenyl]disulfanyl]phenyl]-pyrrolidin-1-yl-methanone

Participants

Reaction Steps

This compound was prepared according to the general method of Example 112 using 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 15 mL of dichloromethane and pyrrolidine (0.63 mL, 7.5 mmol) and triethylamine (1.2 mL, 9 mmol) in 20 mL of dichloromethane, to give 0.75 g of the title compound as a foam, mp 62-63° C.;

Provenance & Evidence