HCID 18928602, compound → HCID 21185130, compound

Participants

Reaction Steps

To a stirred solution of 3-3 (4.6 g, 19 mmol) in THF (50 mL) at ambient temperature was added LiAlH4 (9.4 mL, 9.4 mmol; 1M THF solution). After 1.0 h the reaction was quenched with sat. NaK tartrate solution. The mixture was poured into a EtOAc/H2O mixture. The organic portion was washed with brine, dried (MgSO4) and concentrated to give 3-4 as a yellow viscous oil.

Provenance & Evidence