HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86752440, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 15850735 | HCID 15850735 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86752440 | HCID 86752440 | — |
Reaction Steps
8-5 (497 mg, 1.04 mmol) in 5 mL CH2Cl2 was treated with 5 mL TFA at 0° for 30 min then RT for 10 min. Concentration provided 9-1 as a yellow oil. Rf 0.52 (silica, 10:1:1 ethanol/NH4OH/H2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929120 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-7d435f9886634d1eb2ad6bcfa410c27e |
| Source note | uspto-grants-1999_07 |