HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 10456186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 1-(8-Aminooctyl)-2-butyl-1H-imidazo[4,5-c]quinolin-4-amine | HCID 22344448 | — |
| Product | HCID 10456186 | HCID 10456186 | 48.2% |
Reaction Steps
Using the general method of Example 242, 1-(8-aminooctyl)-2-butyl-1H-imidazo[4,5-c]quinolin-4-amine (1.2 g, 3.26 mmol) was reacted with methanesulfonyl chloride (260 μL, 3.26 mmol) to provide 0.70 g of N-[8-(4-amino-2-butyl-1H-imidazo[4,5-c]quinolin-1-yl)octyl]methanesulfonamide as a tan powder, m.p. 121-124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924293B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-51c289d79264452f9708c7ddcd566cc0 |
| Source note | uspto-grants-2005_08 |