HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66847325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (6S,9S,12S)-12-tert-Butoxycarbonylamino-9-isopropyl-8,11-dioxo-2-oxa-7,10-diaza-bicyclo-[12.2.2]octadeca-1(17),14(18),15-triene-6-carboxylic acid methyl ester | HCID 66847362 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66847325 | HCID 66847325 | — |
Reaction Steps
Methyl ester 66 (0.2 g) was dissolved in 4M HCl in 1,4-dioxane (10 mL). The solution was stirred at rt for 16 h before being concentrated in vacuo to yield a brown solid, 0.17 g, 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434762B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-5f03a6f86da44e0ab43854cc45c8da72 |
| Source note | uspto-grants-2016_09 |