Sodium Bicarbonate → HCID 59064566, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of the compound prepared in Example 3(1) (5.02 g) in allyl alcohol (15 ml), concentrated hydrochloric acid (40 drops) was added, and the mixture was stirred for 30 minutes at 50° C. The reaction mixture was cooled to room temperature, neutralized by adding sodium bicarbonate and extracted with ethyl acetate. The extract was dried over anhydrous magnesium sulfate to give the title compound having the following physical data.

Provenance & Evidence