1-Bromopropane → HCID 22345184, compound

HRID 584058Notes

Reaction equation

HRID 584058 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].Br[CH2:18][CH2:19][CH3:20]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:9][CH2:10][N:11]([CH2:18][CH2:19][CH3:20])[CH2:12][CH2:13]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 78401-BromopropaneHCID 47388041-(4-Methyl-3-nitrophenyl)piperazine

Product 1

HCID 22345184HCID 22345184, compound

Procedure

Beginning with 1-(4-methyl-3-nitro-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 263 (M+, 26), 234 (bp), 191 (19), 70 (84), 56 (40).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-00e2808df31a423fa38e35bfbc3e5cd2
Source dataset
uspto-grants-2005_08
Patent number
US06924374B2

Reaction notes

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