1-Bromopropane → HCID 22345152, compound

HRID 584063Notes

Reaction equation

HRID 584063 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].Br[CH2:18][CH2:19][CH3:20]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][N:11]([CH2:18][CH2:19][CH3:20])[CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 78401-BromopropaneHCID 4738747HCID 4738747, compound

Product 1

HCID 22345152HCID 22345152, compound

Procedure

Beginning with 1-(4-Chloro-3-nitro-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. m.p. 249° C. (HCl); MS m/z (rel. intensity, 70 eV) 283 (M+, 27), 254 (87), 165 (bp), 153 (78), 56 (90).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-1312d33eab4648648e94a66daac1f3cc
Source dataset
uspto-grants-2005_08
Patent number
US06924374B2

Reaction notes

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