1-Bromopropane → HCID 22345208, compound

HRID 584065Notes

Reaction equation

HRID 584065 reaction equation
[F:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.Br[CH2:19][CH2:20][CH3:21]>>[F:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][N:15]([CH2:19][CH2:20][CH3:21])[CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:7]=1

Participants

3

Reactant 2

HCID 78401-BromopropaneHCID 11357080HCID 11357080, compound

Product 1

HCID 22345208HCID 22345208, compound

Procedure

Beginning with 1-(3-fluoro-5-trifluoromethyl-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. m.p. 242° C. (HCl); MS m/z (rel. intensity, 70 eV) 290 (M+, 34), 261 (bp), 218 (22), 190 (20), 70 (37).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-22b1814a21e34c51b19ed8988281cb1d
Source dataset
uspto-grants-2005_08
Patent number
US06924374B2

Reaction notes

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