Allyl bromide → HCID 22345159, compound

HRID 584073Notes

Reaction equation

HRID 584073 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([N:13]2[CH2:18][CH2:17][NH:16][CH2:15][CH2:14]2)[CH:8]=[CH:9][C:10]=1[O:11][CH3:12])(=[O:4])=[O:3].[CH2:19](Br)[CH:20]=[CH2:21]>>[CH2:21]([N:16]1[CH2:15][CH2:14][N:13]([C:7]2[CH:8]=[CH:9][C:10]([O:11][CH3:12])=[C:5]([S:2]([CH3:1])(=[O:3])=[O:4])[CH:6]=2)[CH2:18][CH2:17]1)[CH:20]=[CH2:19]

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 22345160HCID 22345160, compound

Product 1

HCID 22345159HCID 22345159, compound

Procedure

Beginning with 1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine and allylbromide, the title compound was recovered by the procedure described in Example 2: MS m/z (rel. intensity, 70 eV)) 310 (M+, 91), 214 (73), 96 (86), 69 (80), 56 (bp).

Workup

  1. customthe title compound was recovered by the procedure

Sources & evidence

ORD record
ord-7eb210aee5b342afafb1b03aeeb6f7ed
Source dataset
uspto-grants-2005_08
Patent number
US06924374B2

Reaction notes

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