Acrylic Acid → HCID 69792482, compound

HRID 584256Notes

Reaction equation

[C:1]([C:5]1[C:6]([O:29][CH3:30])=[C:7]([C:15]2[C:20]([OH:21])=[CH:19][CH:18]=[C:17]([CH:22]=[CH:23][C:24]([O:26]CC)=[O:25])[CH:16]=2)[CH:8]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:10]=1)([CH3:4])([CH3:3])[CH3:2].C(O)(=O)C=C>>[C:1]([C:5]1[C:6]([O:29][CH3:30])=[C:7]([C:15]2[C:20]([OH:21])=[CH:19][CH:18]=[C:17]([CH:22]=[CH:23][C:24]([OH:26])=[O:25])[CH:16]=2)[CH:8]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:10]=1)([CH3:2])([CH3:3])[CH3:4]

Participants

Reactant 2

HCID 6581Acrylic Acid

HCID 69793956HCID 69793956, compound

Product 1

HCID 69792482HCID 69792482, compound

Procedure

In a manner similar to that of Example 2(h), starting with 1.23 g (3 mmol) of ethyl 3-(3′,5′-di-tert-butyl-6-hydroxy-2′-methoxy-3-biphenylyl)acrylate, 800 mg (69%) of 3-(3′,5′-di-tert-butyl-6-hydroxy-2′-methoxy-3)) -biphenylyl)acrylic acid having a melting point of 166°-7° C. were obtained.

Workup

customwere obtained

Sources & evidence

ORD record: ord-4b42c2c3662d412d869d1c6d88081b07
Source dataset: uspto-grants-2005_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06924388B2

Reaction notes

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