HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triisopropyl borate → 5-[1,3]Dioxolan-2-yl-2-methylphenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triisopropyl borate | HCID 21531 | — |
| Reactant | 1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)- | HCID 11241979 | — |
| Product | 5-[1,3]Dioxolan-2-yl-2-methylphenylboronic acid | HCID 22345636 | — |
Reaction Steps
In a manner similar to that of Example 2(k), by reacting 11.1 g (46 mmol) of 2-(3-bromo-4-methylphenyl)[1,3]dioxolane with 12.3 ml (55 mmol) of triisopropyl borate, 6 g (88%) of product are obtained in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924400B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-d41da316721d4ee38d4763bbf5e49684 |
| Source note | uspto-grants-2005_08 |