HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86596450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Pyridinium hydrochloride | HCID 21584435 | — |
| Reactant | HCID 53432346 | HCID 53432346 | — |
| Product | HCID 86596450 | HCID 86596450 | — |
Reaction Steps
152.0 g (0.460 mol) pentafluorophenyltriethoxysilane, 34 mL (0.460 mol, 54.724 g) thionylchloride and 6.910 g (0.0598 mol) pyridinium hydrochloride are refluxed and stirred for 18 h. Pyridinium hydrochloride is precipitated at −78° C. and the solution is filtrated. Pentafluorophenylchlorodiethoxysilane is isolated by vacuum distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924384B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-30d1170868444444852be8dbd54e3b72 |
| Source note | uspto-grants-2005_08 |