HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium borohydride → 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium borohydride | HCID 4311764 | — |
| Edukt | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzaldehyde | HCID 10829743 | — |
| Produkt | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol | HCID 57315820 | 93,9% |
Reaktionsschritte
In substantially the same manner in Reference Example 93, 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzaldehyde (6.47 g) was reduced by sodium borohydride (760 mg) to obtain 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)benzyl alcohol (6.11 g, yield 93%) as crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06924300B2 |
| Quelldatensatz | uspto-grants-2005_08 |
| ORD ID | ord-fa32c5983ed647a8bc97a67e647808d5 |
| Quellennotiz | uspto-grants-2005_08 |