Methanesulfonamide → HCID 69780760, compound

HRID 584583Notes

Reaction equation

HRID 584583 reaction equation
[C:1]1([C:7]2[CH2:8][O:9][C:10]3[C:15]([C:16]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25]([OH:27])=O)=[CH:19][CH:18]=2)=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:28][S:29]([NH2:32])(=[O:31])=[O:30]>>[C:1]1([C:7]2[CH2:8][O:9][C:10]3[C:15]([C:16]=2[C:17]2[CH:22]=[CH:21][C:20]([CH:23]=[CH:24][C:25]([NH:32][S:29]([CH3:28])(=[O:31])=[O:30])=[O:27])=[CH:19][CH:18]=2)=[CH:14][CH:13]=[CH:12][CH:11]=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Procedure

Prepared from the coupling of 3d and methylsulfonamide by the method described in Procedure 1, Method A. Yield (35%); ESI m/z: 430 (M−H−, 100%).

Workup

  1. customYield (35%)

Sources & evidence

ORD record
ord-b3d4a34b7efd4416953a477c7ec83dd2
Source dataset
uspto-grants-2005_08
Patent number
US06927224B2

Reaction notes

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