HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-6-ethoxyquinoline-3-carbaldehyde → 2-Chloro-6-ethoxyquinoline-3-carbaldehyde-O-methyl-oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-6-ethoxyquinoline-3-carbaldehyde | HCID 788658 | — |
| Reactant | HCID 22341071 | HCID 22341071 | — |
| Product | 2-Chloro-6-ethoxyquinoline-3-carbaldehyde-O-methyl-oxime | HCID 73884070 | — |
Reaction Steps
To a solution of 2-chloro-6-ethoxyquinoline-3-carbaldehyde (0.235 g, 1.0 mmol) in ethanol O-methylhydroxylamine hydrochloride (0.10 g, 1.1 mmol) was added. The reaction mixture was heated to reflux for 0.5 hours. After cooling to room temperature the precipitated compound was filtered and dried. Yield 180 mg. M.p. 142-4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927214B1 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-a54f64eba8e247f0ae17a36478d376c7 |
| Source note | uspto-grants-2005_08 |