HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,3-Trifluoro-1-phenylpropane-1,2-dione hydrate → 6,7-Dinitro-2-phenyl-3-trifluoromethylquinoxaline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,3-Trifluoro-1-phenylpropane-1,2-dione hydrate | HCID 2781162 | — |
| Reactant | 4,5-Dinitrobenzene-1,2-diamine | HCID 4441903 | — |
| Product | 6,7-Dinitro-2-phenyl-3-trifluoromethylquinoxaline | HCID 22341147 | — |
Reaction Steps
The title compound was prepared from 4,5-dinitro-1,2-phenylenediamine (890 mg, 4.5 mmol) and 3,3,3-trifluoro-1-phenyl-1,2-propanedione hydrate (1 g, 4.9 mmol) similarly as described in example 144.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927214B1 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-c7f2a84afb4e4a69a69d6ac430f2a9cf |
| Source note | uspto-grants-2005_08 |