Ethyl 3-bromobenzoate → HCID 15382496, compound

HRID 584932Notes

Reaction equation

HRID 584932 reaction equation
Br[C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[C:5]([O:7][CH2:8][CH3:9])=[O:6].[CH:13]([C:15]1[CH:20]=[CH:19][C:18](B(O)O)=[CH:17][CH:16]=1)=[O:14]>>[CH:13]([C:15]1[CH:20]=[CH:19][C:18]([C:2]2[CH:12]=[CH:11][CH:10]=[C:4]([C:5]([O:7][CH2:8][CH3:9])=[O:6])[CH:3]=2)=[CH:17][CH:16]=1)=[O:14]

Participants

3

Reactant 2

HCID 90488Ethyl 3-bromobenzoateHCID 5910734-Formylphenylboronic Acid

Product 1

HCID 15382496HCID 15382496, compoundYield 60%

Procedure

In a manner similar to that of Example 1(e), by reacting 12.6 ml (79 mmol) of ethyl 3-bromobenzoate with 15 g (100 mmol) of 4-formylbenzene boronic acid, 12 g (60%) of the expected product are obtained.

Sources & evidence

ORD record
ord-c76154cbf1f940c98d2c4cc63f149921
Source dataset
uspto-grants-2005_08
Patent number
US06927228B2

Reaction notes

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