HCID 86591263, compound → HCID 10299501, compound

HRID 584951Notes

Reaction equation

HRID 584951 reaction equation
[O:1]=[C:2]1[NH:6][C:5](=[O:7])[C:4](=[CH:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[C:17]([CH2:21][N:22]([CH3:34])[C:23](=[O:33])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:16]=3)=[CH:11][CH:10]=2)[S:3]1>O1CCOCC1>[O:1]=[C:2]1[NH:6][C:5](=[O:7])[CH:4]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([C:15]3[CH:20]=[CH:19][CH:18]=[C:17]([CH2:21][N:22]([CH3:34])[C:23](=[O:33])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:16]=3)=[CH:11][CH:10]=2)[S:3]1

Participants

3

Reactant 1

HCID 86591263HCID 86591263, compound

Product 1

HCID 10299501HCID 10299501, compoundYield 65%

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

In a manner similar to that of Example 1(g), starting with 460 mg (1 mmol) of N-[4′-(2,4-dioxothiazolidin-5-ylidenemethyl)biphenyl-3-ylmethyl]-N-methyldecanamide in 8 ml of dioxane, 300 mg (65%) of the desired product are obtained in the form of a film.

Sources & evidence

ORD record
ord-870cab7654de4e40ad9049c40eecc955
Source dataset
uspto-grants-2005_08
Patent number
US06927228B2

Reaction notes

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