HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitroethane → Ethyl 8,9-dimethoxy-3-methyl-2-(3-nitrophenyl)-5,6-dihydropyrrolo[2,1-a]isoquinoline-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | 3-Nitrobenzaldehyde | HCID 7449 | — |
| Reactant | ethyl 2-(6,7-dimethoxy-3,4-dihydro-2H-isoquinolin-1-ylidene)acetate | HCID 70037591 | — |
| Product | Ethyl 8,9-dimethoxy-3-methyl-2-(3-nitrophenyl)-5,6-dihydropyrrolo[2,1-a]isoquinoline-1-carboxylate | HCID 10181470 | — |
Reaction Steps
Following the procedure described in Example 1, ethyl (6,7-dimethoxy-3,4-dihydro-1(2H)-isoquinolinylidene)-ethanoate (Example III.1), 3-nitro-benzaldehyde, and nitroethane were reacted to give ethyl 8,9-dimethoxy-3-methyl-2-(3-nitrophenyl)-5,6-dihydro-pyrrolo[2,1-a]-isoquinoline-1-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06930114B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-7240b05bd52042738fd217bd07c3a432 |
| Source note | uspto-grants-2005_08 |