Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | HCID 22339565 | HCID 22339565 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22339462 | HCID 22339462 | — |
Reaction Steps
To a cooled (0° C.), stirred solution of 2-[3,5-dichloro-4-(3-formyl-4-methoxy-phenoxy)-phenyl]-2H-[1,2,4]triazine-3,5-dione (0.4 g) in dichloromethane (10 mL) was added 1M boron trichloride in dichloromethane (4 mL). The resulting orange slurry was stirred at ambient temperature for 5 h, ice added and the reaction stirred an additional 1 h. The two phase solution was diluted into ethyl acetate and washed with water, brine, dried (Na2SO4), concentrated in vacuo to afford the title compound of Step B as an off-white solid, 0.4 g (m.p. 146-150° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06930107B2 |
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| Source dataset | uspto-grants-2005_08 |
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| ORD ID | ord-8db8284acf164afaad40dd55e831db88 |
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| Source note | uspto-grants-2005_08 |
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