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HRID 58516作成日:2026年10月25日

Methane → Biphenyl

https://huagongshe.com/reaction/58516

反応式

関与物質

役割名称HCID仕込み量
反応物MethaneHCID 297—
反応物BiphenylHCID 7095—
反応物O-PhenylenediamineHCID 7243—
溶媒N-methyl-2-pyrrolidoneHCID 13387—
生成物BiphenylHCID 7095—
生成物Phenylenediamine carbon blackHCID 131733384—

反応手順

More specifically, an intermediate transfer coating dispersion was prepared by providing a mixture of Special Carbon Black 4, available from Orion Chemicals, the polyamic acid of biphenyl tetracarboxylicdianhydride/phenylenediamine in N-methyl-2-pyrrolidone (NMP) (about 17 weight percent of solids), and not that readily soluble in the NMP solvent the leveling agent NOVEC™ FC-4432, a fluoro surfactant available from 3M, and which mixture was stirred and subjected to ball milling with 2 millimeter stainless steel shots via an Attritor grinding mill for 18 hours. There resulted a coating dispersion of the polyamic acid of biphenyl tetracarboxylicdianhydride/phenylenediamine/carbon black/leveling agent dispersed in NMP, where the weight ratio of polyamic acid of biphenyl tetracarboxylicdianhydride/phenylenediamine/carbon black/leveling agent was 88.8/11/0.2, and which dispersion was filtered with a 20 micron Nylon cloth filter.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09436137B2
出典データセットuspto-grants-2016_09
ORD IDord-b0572acb3e344218a2dfd3ed26d5afab
出典メモuspto-grants-2016_09