HRID585169
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
500 ml of water and 40 g of KOH are charged into a 1 liter glass flask, containing 43 g of 2-ethoxycarbonyl-2-(2-oxopropyl)-α-tetralone (XV), 65% purity, obtained as described above. The mixture is then heated to reflux temperature for 10 hours, the reaction trend being followed by means of TLC.
WORKUP
后处理
- customobtained
- temperatureThe mixture is then heated
- temperatureto reflux temperature for 10 hours