Potassium Hydroxide → HCID 10976167, compound

HRID 585169Notes

Reaction equation

HRID 585169 reaction equation
[OH-].[K+].O=[C:4]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[CH2:7][CH2:6][C:5]1([CH2:19][C:20](=[O:22])[CH3:21])C(OCC)=O>O>[CH:21]1[C:20](=[O:22])[CH2:19][CH:5]2[CH2:6][CH2:7][C:8]3[C:13](=[CH:12][CH:11]=[CH:10][CH:9]=3)[C:4]=12

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 22340242HCID 22340242, compound

Product 1

HCID 10976167HCID 10976167, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

500 ml of water and 40 g of KOH are charged into a 1 liter glass flask, containing 43 g of 2-ethoxycarbonyl-2-(2-oxopropyl)-α-tetralone (XV), 65% purity, obtained as described above. The mixture is then heated to reflux temperature for 10 hours, the reaction trend being followed by means of TLC.

Workup

  1. customobtained
  2. temperatureThe mixture is then heated
  3. temperatureto reflux temperature for 10 hours

Sources & evidence

ORD record
ord-95b79f2d6f7d485697a2e540d9e20684
Source dataset
uspto-grants-2005_08
Patent number
US06930158B2

Reaction notes

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