1-Hexanethiol → 9-[1-(3,4-Dimethoxybenzoyl)-2-[5-(hexylthio)pentyl]-1,2,3,4-tetrahydro-4-quinolinyl]-9H-carbazole

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Reaction Steps

Starting with 5-[4-(9H-9-carbazolyl)-1-(3,4-dimethoxybenzoyl)-1,2,3,4-tetrahydro-2-quinolinyl]-1-pentanol (0.08 g, 0.15 mmol) prepared in Example 135 and n-hexylmercaptan (0.3 ml), the same procedure as shown in Example 136 was repeated to give the titled compound (0.01 g, yield: 7%) as a white crystal (cis:trans=6:1).

Provenance & Evidence