HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetamide → HCID 21927943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | HCID 533795 | HCID 533795 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21927943 | HCID 21927943 | — |
Reaction Steps
Cyanoacetamide was stirred with sodium ethoxide in ethanol for 30 minutes. 2-Cyano-3-pyridin-3-yl-but-2-enoic acid ethyl ester was added and allowed to sit for 16 hours. The solution was acidified to pH 4 and partially concentrated under reduced pressure, causing precipitation of product. The product was filtered and allowed to dry. MS (ESI+) for C13H10N4O2 m/z 255.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06933304B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-192c753dd91d4ca8a1dbb2d80f01a5f3 |
| Source note | uspto-grants-2005_08 |