HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloroformate → HCID 69619626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | HCID 20824479 | HCID 20824479 | — |
| Product | HCID 69619626 | HCID 69619626 | 90.2% |
Reaction Steps
By a similar reaction operation as in Starting Material Synthetic Example 4 using 5-amino-2,3,4,5-tetrahydro-1-benzothiepine-8-carboxylic acid methyl ester (2.50 g) and benzyloxycarbonyl chloride (2.69 g), the objective 5-(benzyloxycarbonylamino)-2,3,4,5-tetrahydro-1-benzothiepine-8-carboxylic acid methyl ester (3.53 g) was obtained as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06933305B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-a9e90d87db7c4082a338428baa45ceef |
| Source note | uspto-grants-2005_08 |