HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → Methyl 4-hydroxychroman-7-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Methyl 4-oxochroman-7-carboxylate | HCID 11769654 | — |
| Product | Methyl 4-hydroxychroman-7-carboxylate | HCID 20824498 | 106.1% |
Reaction Steps
By a similar reaction operation as in Starting Material Synthetic Example 1 using 4-oxochromane-7-carboxylic acid methyl ester (1.4 g) synthesized according to a known method and sodium borohydride (0.26 g), the objective 4-hydroxychromane-7-carboxylic acid methyl ester (1.5 g) was obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06933305B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-ba7fa613a0b843f18db4abd343f2cb2b |
| Source note | uspto-grants-2005_08 |