HRID586056

反应详情

EQUATION

反应方程式

HRID 586056 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-(4-Chlorophenyl)-2-methylpropanoic acid (3.85 g, 19.4 mmol) in toluene (5 mL) and thionyl chloride (5.00 g, 3.1 mL) was heated at 80° C. for 2 hours. The mixture was cooled and concentrated under reduced pressure to provide the title compound.

WORKUP

后处理

  1. temperatureThe mixture was cooled
  2. concentrationconcentrated under reduced pressure