HCID 9815198, compound → HCID 9857886, compound

Participants

Reaction Steps

1H NMR (400 MHz, CDCl3) δ 2.72 (3H, s), 7.50 (1H, td, J 7.6, 1.3 Hz), 7.59-7.67 (3H, m), 7.70 (1H, td, J 7.7, 1.4 Hz), 7.82 (1H, dd, J 7.8, 1.0 Hz), 8.14 (1H, dt, J 7.6, 1.6 Hz), 8.29 (2H, m), 8.37 (1H, s); MS (ES+) m/z 312 [M+H]+. 3′-(3-Methylimidazo[1,2-b][1,2,4]triazin-7-yl)biphenyl-2-carbonitrile: mp 211-216° C. (CH2Cl2-EtOAc-isohexane); 1H NMR (400 MHz, CDCl3) δ 2.73 (3H, s), 7.50 (1H, td, J 7.6, 1.3 Hz), 7.59-7.66 (3H, m), 7.70 (1H, td, J 7.7, 1.4 Hz), 7.82 (1H, dd, J 7.8, 1.4 Hz), 8.10 (1H, dt, J 7.6, 1.5 Hz), 8.29 (2H, t, J 1.4 Hz), 8.26 (1H, s), 8.36 (1H, s); MS (ES+) m/z 312 [M+H]+.

Provenance & Evidence