HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetanilide → HCID 9862611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetanilide | HCID 904 | — |
| Reactant | (4-chlorophenyl)(pyridin-3-yl)methanol | HCID 240724 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 9862611 | HCID 9862611 | 100% |
Reaction Steps
A mixture of α-(4-chlorophenyl)-3-pyridinemethanol (0.364 mol) and N-phenyl acetamide (0.364 mol) in HOAc (360 ml) and H2SO4 36N (38.6 ml) was stirred and refluxed for 6 days. The solvent was evaporated, yielding 122.6 g (±)-N-[4-[(4-chloro-phenyl)(3-pyridinyl)methyl]phenyl]acetamide (compound 673).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936626B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-87a1c25190ff4ba88bcc981734f11bc3 |
| Source note | uspto-grants-2005_08 |