HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethylbenzaldehyde → tert-Butyl-[5-(2,5-dimethyl-phenyl)-imidazo[1,2-b][1,2,4]triazol-6-yl]-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethylbenzaldehyde | HCID 22015 | — |
| Reactant | Tert-Butyl isocyanide | HCID 23577 | — |
| Reactant | HCID 178418311 | HCID 178418311 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | tert-Butyl-[5-(2,5-dimethyl-phenyl)-imidazo[1,2-b][1,2,4]triazol-6-yl]-amine | HCID 22335585 | — |
Reaction Steps
Compound 49 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 3-amino-1,2,4-triazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) tert-butylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) 2,5-dimethylbenzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%) in a substance library.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936631B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-ec8961cb9f9d47f9949857cce823f1d5 |
| Source note | uspto-grants-2005_08 |