HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 86595798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 86595795 | HCID 86595795 | — |
| Reactant | HCID 86595796 | HCID 86595796 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86595798 | HCID 86595798 | 42% |
| Product | HCID 86595799 | HCID 86595799 | 42% |
Reaction Steps
Following a procedure similar to that for the preparation of Intermediates 8a and 9a but using intermediate 7b as the starting material and 10% EtOAc in hexane as normal phase HPLC eluent afforded Intermediate 10b (49 mg, 42% yield) and Intermediate 11b (48 mg, 42% yield) from 7b as colorless oils:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936636B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-b5af6ac0e2114313a23cad5a33f8959f |
| Source note | uspto-grants-2005_08 |