HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 59981114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 69737302 | HCID 69737302 | — |
| Reactant | HCID 86759826 | HCID 86759826 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 59981098 | HCID 59981098 | 41% |
| Product | HCID 59981114 | HCID 59981114 | 45% |
Reaction Steps
Following a procedure similar to that for the preparation of Intermediates 41 and 42 but using Intermediate 40a as the starting material and using 10% EtOAc in hexane as normal phase HPLC eluent afforded Intermediate 43a (25 mg, 45% yield) and Intermediate 44a (23 mg, 41% yield) as colorless oils:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936636B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-361bca9f39114c01b5dbda2985dca5ad |
| Source note | uspto-grants-2005_08 |