HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 86595806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 69737497 | HCID 69737497 | — |
| Reactant | HCID 86759826 | HCID 86759826 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86595806 | HCID 86595806 | 43% |
| Product | HCID 86595807 | HCID 86595807 | 41% |
Reaction Steps
Following a procedure similar to that for the preparation of Intermediates 41 and 42 but using Intermediate 40b as the starting material, ethyl iodide as the alkylating reagent and using 10% EtOAc in hexane as normal phase HPLC eluent afforded Intermediate 43b (59 mg, 43% yield) and Intermediate 44b (56 mg, 41% yield) as colorless oils:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936636B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-5e3dc03e93ce4049b6ef943fd840ef1c |
| Source note | uspto-grants-2005_08 |