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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 586681Generated: November 1, 2026

Iodoethane → HCID 86595806, compound

https://huagongshe.com/reaction/586681

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIodoethaneHCID 6340—
ReactantEthyl AcetateHCID 8857—
ReactantHCID 69737497HCID 69737497—
ReactantHCID 86759826HCID 86759826—
SolventHexaneHCID 8058—
ProductHCID 86595806HCID 8659580643%
ProductHCID 86595807HCID 8659580741%

Reaction Steps

Following a procedure similar to that for the preparation of Intermediates 41 and 42 but using Intermediate 40b as the starting material, ethyl iodide as the alkylating reagent and using 10% EtOAc in hexane as normal phase HPLC eluent afforded Intermediate 43b (59 mg, 43% yield) and Intermediate 44b (56 mg, 41% yield) as colorless oils:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06936636B2
Source datasetuspto-grants-2005_08
ORD IDord-5e3dc03e93ce4049b6ef943fd840ef1c
Source noteuspto-grants-2005_08