5-Chloro-2-nitroanisole → HCID 10301601, compound

HRID 586773Notes

Reaction equation

HRID 586773 reaction equation
[NH2:1][C:2](=[N:8][C:9]1[CH:14]=[CH:13][C:12]([N:15]2[CH2:20][CH2:19][N:18]([C:21]([NH:23][CH2:24][CH2:25][CH2:26][CH2:27][CH:28]3[CH2:32][CH2:31][S:30][S:29]3)=[O:22])[CH2:17][CH2:16]2)=[C:11](C)[CH:10]=1)[C:3]1[S:4][CH:5]=[CH:6][CH:7]=1.ClC1C=CC([N+]([O-])=O)=[C:39]([O:41]C)C=1>>[NH2:1][C:2](=[N:8][C:9]1[CH:10]=[CH:11][C:12]([N:15]2[CH2:16][CH2:17][N:18]([C:21]([NH:23][CH2:24][CH2:25][CH2:26][CH2:27][CH:28]3[CH2:32][CH2:31][S:30][S:29]3)=[O:22])[CH2:19][CH2:20]2)=[CH:13][C:14]=1[O:41][CH3:39])[C:3]1[S:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 811105-Chloro-2-nitroanisoleHCID 10185551HCID 10185551, compound

Product 1

HCID 10301601HCID 10301601, compoundYield 4%

Procedure

The experimental protocol used is the same as that described for the compound of Example 6, 5-chloro-2-nitroanisole replacing 2-fluoro-5-nitrotoluene. A pale yellow foam is obtained (yield 4%).

Workup

  1. customA pale yellow foam is obtained (yield 4%)

Sources & evidence

ORD record
ord-23ee6cdb3c1c4f1d82a7f7140a70341e
Source dataset
uspto-grants-2005_08
Patent number
US06936715B2

Reaction notes

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