HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 131725116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 131725107 | HCID 131725107 | — |
| Product | HCID 131725116 | HCID 131725116 | 40% |
Reaction Steps
Using a procedure analogous to Example 26, the product from Example 14 (120 mg, 0.150 mmol) was treated with pivaloyl chloride (21.7 mg, 1.2 eq) to provide the title barbituric acid (45.0 mg, 40%). MS found: (M+H)+=544.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936620B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-347cb9d3682e4778865635b1a4c7d408 |
| Source note | uspto-grants-2005_08 |