HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 131725117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 131725107 | HCID 131725107 | — |
| Product | HCID 131725117 | HCID 131725117 | 37% |
Reaction Steps
Using a procedure analogous to Example 26, the product from Example 14 (120 mg, 0.150 mmol) was treated with methanesulfonyl chloride (24.0 mg, 1.4 eq) to provide the title barbituric acid (42.0 mg, 37%). MS found: (M+H)+=538.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936620B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-ce45b69d756d45d29f4f8d9577538235 |
| Source note | uspto-grants-2005_08 |