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HRID587139

反应详情

EQUATION

反应方程式

HRID 587139 的结构方程式

REACTANTS

反应物

3
结构：Clc1ncnc(Cl)n1
HCID17810

2,4-Dichloro-1,3,5-triazine

C3HCl2N3

结构：Nc1cccc(CCS(N)(=O)=O)c1
HCID58236871

未命名化合物

结构：NS(=O)(=O)Cc1cccc(Nc2ncnc(Cl)n2)c1
HCID86679822

未命名化合物

PRODUCTS

生成物

1
结构：NS(=O)(=O)CCc1cccc(Nc2ncnc(Cl)n2)c1
HCID86679825

未命名化合物

PROCEDURE

实验过程

A4 was prepared following the general procedure reported for A1 using 2,4-dichloro-1,3,5-triazine and 2-(3-aminophenyl)ethanesulfonamide A3 as reacting agents. The crude product was purified by flash chromatography on silica gel (DCM/MeOH=100:0 to 4:1) to yield the desired product A5 (54%, 65% purity) as a brown solid. MS (ES) C11H12ClN5O2S requires: 313. found: 314 (M+H)+.

WORKUP

后处理

  1. customThe crude product was purified by flash chromatography on silica gel (DCM/MeOH=100:0 to 4:1)