HCID 18765177, compound → HCID 60197602, compound

HRID 587171Notes

Reaction equation

HRID 587171 reaction equation
Cl[C:2]1[N:7]=[CH:6][N:5]=[C:4]([NH:8][C:9]2[CH:10]=[C:11]([CH2:15][S:16]([NH2:19])(=[O:18])=[O:17])[CH:12]=[CH:13][CH:14]=2)[N:3]=1.Cl.[N:21]1[C:26]2[CH2:27][CH2:28][NH:29][CH2:30][C:25]=2[CH:24]=[N:23][CH:22]=1>>[N:21]1[C:26]2[CH2:27][CH2:28][N:29]([C:2]3[N:7]=[CH:6][N:5]=[C:4]([NH:8][C:9]4[CH:10]=[C:11]([CH2:15][S:16]([NH2:19])(=[O:18])=[O:17])[CH:12]=[CH:13][CH:14]=4)[N:3]=3)[CH2:30][C:25]=2[CH:24]=[N:23][CH:22]=1

Participants

3

Reactant 2

HCID 18765177HCID 18765177, compoundHCID 866798223-[(4-Chloro-1,3,5-triazin-2-yl)amino]benzenemethanesulfonamide

Product 1

HCID 60197602HCID 60197602, compound

Procedure

B39 was prepared following the general procedure reported for B10 using A1 and 5,6,7,8-tetrahydropyrido[4,3-d]pyrimidine hydrochloride; yield: 29.7 mg (7%), pale yellow solid. MS (ES) C17H18N8O2S requires: 398. found: 399 (M+H)+.

Workup

  1. customB39 was prepared

Sources & evidence

ORD record
ord-a7c9b58ff01c49a29a88edf8c0be760c
Source dataset
uspto-grants-2016_01
Patent number
US09226929B2

Reaction notes

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