HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86675232, compound → HCID 86675231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86675232 | HCID 86675232 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 86675231 | HCID 86675231 | 67.8% |
Reaction Steps
A solution of (E)-ethyl 5-(3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-1-en-1-yl)-2-(1H-1,2,4-triazol-1-yl)benzoate (0.2 g, 0.4 mmol) in 6 N HCl (10 mL) was stirred at 100° C. for 18 h. The reaction was cooled to ambient temperature, resulting in a white solid precipitate. The precipitate was filtered to afford the title compound as a white solid (0.12 g, 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09226501B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-0b110a338e7b460387f5c60e140b199e |
| Source note | uspto-grants-2016_01 |