HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(2-Methoxyphenyl)piperazine → Nan 190
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Edukt | N-(4-Bromobutyl)phthalimide | HCID 93575 | — |
| Edukt | 1-(4-Aminobutyl)-4-(2-methoxyphenyl)piperazine | HCID 10999903 | — |
| Produkt | Nan 190 | HCID 4431 | 84,3% |
Reaktionsschritte
4-[4-(2-methyloxyphenyl)piperazinyl]butylamine: according to the method of claim 1, N-(4-bromobutyl)phthalimide and 2-methyloxyphenyl-piperazine was used in reaction to produce N-{4-[4-(2-methyloxyphenyl)piperazinyl]butyl}phthalimide, which was then reacted with hydrazine hydrate. The yield was: 84.3%. Hydrochloride salt had a mp: 173-175° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09227944B2 |
| Quelldatensatz | uspto-grants-2016_01 |
| ORD ID | ord-f548bb3f3aa44d33a8ea26ca47e64291 |
| Quellennotiz | uspto-grants-2016_01 |