HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopropane → HCID 59419921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| Reactant | Ethyl 3,4-dimethoxyphenylacetate | HCID 87441 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Product | HCID 59419921 | HCID 59419921 | — |
Reaction Steps
For Step 1, (3,4-dimethoxy-phenyl)-acetic acid ethyl ester was substituted for (3,4-Dimethoxyphenyl)acetonitrile, ethyl chloroformate was substituted for 2-bromopropane and lithium diisopropylamide (LDA) was substituted for NaHMDS. For Step 2, sodium hydride was substituted for NaHMDS.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227918B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-fe273c7d3ece4bedade145579cbc2a75 |
| Source note | uspto-grants-2016_01 |