HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(2-(methylamino)ethyl)benzoate → Ethyl 4-(2-((4-(3,4-dimethoxyphenyl)-4-(methoxycarbonyl)-5-methylhexyl)(methyl)amino)ethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(2-(methylamino)ethyl)benzoate | HCID 59419931 | — |
| Reactant | Methyl 5-chloro-2-(3,4-dimethoxyphenyl)-2-isopropylpentanoate | HCID 59419939 | — |
| Product | Ethyl 4-(2-((4-(3,4-dimethoxyphenyl)-4-(methoxycarbonyl)-5-methylhexyl)(methyl)amino)ethyl)benzoate | HCID 25131316 | — |
Reaction Steps
Reaction of 1e with 2c produced 3w. MS found M+H=500. The oxalate salt of 3w was recrystallized from ethyl acetate; mp 121-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227918B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-e2099279929a46818900aff177e0f27e |
| Source note | uspto-grants-2016_01 |